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Cystobactamids 920-1 and 920-2: Assignment of the Constitution and Relative Configuration by Total Synthesis.
Planke, Therese Moreno, María Hüttel, Stephan Fohrer, Jörg Gille, Franziska Norris, Matthew D Siebke, Maik Wang, Liangliang Kirschning, Andreas
Planke, Therese
Moreno, María
Hüttel, Stephan
Fohrer, Jörg
Gille, Franziska
Norris, Matthew D
Siebke, Maik
Wang, Liangliang
Kirschning, Andreas
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2019-03-01
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Abstract
Total synthesis of cystobactamid 920-1 and its epimer has allowed an unambiguous assignment of the relative and absolute configuration of the natural product. A careful structural analysis of each isomer using both NMR and computational techniques also prompted a constitutional revision of the structures originally reported for cystobactamids 920-1 and 920-2, and has provided further insight into the unique conformational preferences of the cystobactamid family
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Org Lett. 2019 Mar 1;21(5):1359-1363. doi: 10.1021/acs.orglett.9b00058. Epub 2019 Feb 8.
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en
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1523-7052
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Attribution-NonCommercial-ShareAlike 4.0 International